Broadening the field of ceramic components by joint and interactive research on EDM machining technology, noval ceramic materials based on nano-powders made by SHS and design methodology

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  The MONCERAT project aims the research in the development of ceramic materials that can optimally be machined by EDM. The uniqueness of this project is to work on the development of the material as well as on the development of the EDM machining process. The materials to be developed should fulfil functional requirements such as mechanical properties (strength, toughness,...) as well as requirements related to the machineabilty by EDM. Further, the project aims to study how material properties of ceramics produced by EDM can be integrated into the design phase.

  The development of a proper EDM technology (generator, machining strategy,...) for ceramics requires a good knowledge of the material removal mechanisms. It is known that in case of steel and cemented carbides (WC-Co), the material removal is based on melting and evaporation. When machining ceramics melting and evaporation still may occur. However, other material removal mechanisms could occur as well, such as sublimation or removal of solid particles due to thermal shocks and fall out of structural elements due to melting of the binder phase. Different material removal principles can occur at the same time. Whether the one or the other mechanism is more dominant depends on the material (microstructure,...) and the EDM process conditions (generator settings, type of dielectric, ...). The exact material removal mechanism is not known for all the materials envisaged in this project. Therefore, research is required in order to understand the relation between the ceramic material and the EDM process. This basic understanding will allow to define an optimal EDM process strategy for the machining of existing materials and to develop both new materials and related EDM process technology for newer ceramic materials.

  The MONCERAT project will focus on three major classes of materials, non-oxide ceramics with none or a minor addition of sinter additives, ZrO2-containing electro-conductive ceramic matrix composites and non-oxide-based cermets with a metal binder. The three classes of material will span a range of hardness, toughness, density and strength. The role of the mechanical properties will be variable depending on the envisaged industrial application. For example, pure non-oxide ceramics are not expected to perform well as punching tools because of their lower strength and toughness, whereas the zirconia-containing ceramics on the other hand should perform well from a strength and fracture toughness point of view. In addition, it is also important to consider a range of chemistries for the EDM material removal mechanism and the corrosion resistance.

  How the microstructure of the ceramic material influences the EDM process (and vice versa) has to be studied in detail within the MONCERAT project. The microstructure is strongly influenced, not only by the composition of the ceramic material (influenced by type of powders, powder properties, additives,...) but also by the sintering process (temperature cycle) and how the powders are produced. Further, the EDM process has on his turn a strong influence on the surface and sub-surface quality. The high temperatures (due to the EDM discharges) influences the metallurgical structure of the upper-layers. For example, it is known that the use of nano-powders for carbide material, which initially increases the strength of the ceramic material, can result in a higher chance for crack formation during the EDM process, finally resulting in a shorter life time of the ceramic component. How the EDM process influences the surface and sub-surface quality of ceramic materials has to be studied in detail within this research project. The production of non-oxide ceramics without binder requires different temperature cycles during sintering (much higher temperatures will be needed). These higher temperatures can again influence the grain growth during sintering which is not beneficial for the strength of the ceramic material. Research to understand the metallurgical phenomena is needed and is an important objective of this project.

  The project aims further to study the SHS process (Self propagating High temperature Synthesis) for the economic production of high quality nano-powders. The SHS process, for the production of powders, has not been studied in detail at this time. This technique offers great potential and lots of possibilities for the production of non oxide ceramic powders which can be used pure or as a binder material for other - non conductive- ceramic materials. By this, electro-conductive ceramic grades can be attained. The principle of SHS reactions is the elaboration of materials using very exothermic chemical reactions, which are auto-propagated without supplying external energy. The combustion reaction is initiated by supplying a short intense burst of energy, like an electrical spark or a laser beam, at the reactant mixture. The propagation of the combustion reaction is generally comprised between 10-4 and 0.15 m/s and local temperatures can reach values between 1800-3700°C in the reaction zone.

  Looking to the end-users, there is need to have more advanced software systems for the design of ceramic components. The MONCERAT project aims to investigate how these design systems can take the realistic properties of the ceramic material machined by EDM into account. This means that the influence of the EDM process on for example the strength and the tool life of the ceramic component has to be taken into account.

The scientific objectives can be summarised as follows:

·         Study of the sintering parameters, powder material and additives on the final properties of the ceramic material (strength, toughness, ...) as well as the machineability by EDM (by Milestone 3)

·         Detailed investigation of the SHS process with respect to the production of high quality nano-powders. (by Milestone 3)

·         To have a better understanding on the EDM removal mechanism active in the machining of ceramic material. It is aimed to find relation ships between the removal mechanism and the microstructure of the ceramic material. This knowledge is essential for the development of "ideal" ceramic materials and the development of a proper EDM technology. (by Milestone 3)

·         Study of new generator technologies (different pulse shapes, higher currents,...) for the machining of ceramic material. (by Milestone 2)

·         A strong research co-operation between developers of ceramic material and EDM machine builders. (whole of the project)

·         Study on how to integrate the properties of ceramic components made by EDM in the design phase. (by Milestone 2)


The technological objectives (quantifiable and measurable) of the project are as follow:

·         Development of novel ceramic materials that meet the end-users requirements of strength, toughness,... and which can be machined by EDM. (non-oxide ceramics by Milestone 2; non-oxide based cermets and ceramic matrix composites by Milestone 3)

·         More economical production of high quality nano-powders using the SHS process. (nitride powders by Milestone 2; carbide powders by Milestone 3)

·         Development of a prototype EDM generator for the machining (wire EDM, die sinking,...) of ceramic material. (by Milestone 3)

·         Development of a software tool for the design of ceramic components taking the properties of ceramic material machined by EDM into account. (by Milestone 2)

·         Design of the correct interfaces between the ceramic part and its metal surroundings. (by Milestone 2)


  Finally, the uniqueness of the MONCERAT project is the strong co-operation between ceramic material producers, EDM machine builders and potential users of ceramic materials in order to extend the fundamental knowledge, needed to developed the ceramic materials of the future, that optimally can be shaped by EDM.


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Last update: 12/02/04